Epoxy curing agent Knowledge 4-Dimethylaminobenzaldehyde 4-Dimethylaminobenzaldehyde

4-Dimethylaminobenzaldehyde 4-Dimethylaminobenzaldehyde

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P-Dimethylaminobenzaldehyde Structural Formula

Structural formula

Business number 02H5
Molecular formula C9H11NO
Molecular weight 149.19
label

p-dimethylaminobenzaldehyde,

p-Dimethylaminobenzene aldehyde,

p-dimethylaminobenzaldehyde,

4-N,N-dimethylaminobenzaldehyde,

N,N-dimethyl-4-aminobenzaldehyde,

p-(N,N-dimethyl)benzaldehyde,

4-Dimethylaminobenzaldehyde,

p-dimethylaminobenzaldehyde,

(CH3)2NC6H4CHO,

4-(Dimethylamino)-benzaldehyd,

4-Formyl-N,N-dimethylaniline,

Benzaldehyde, p-(dimethylamino)-,

Benzaldehyde,-(dimethylamino)-,

Dimethylaminobenzenecarbonal,

N,N-Dimethyl-4-formylaniline,

P-(Dimethylamino)-benzaldehyd,

p-(N,N-Dimethylamino)benzaldehyde

Numbering system

CAS number:100-10-7

MDL number:MFCD00003381

EINECS number:202-819-0

RTECS number:CU5775000

BRN number:606802

PubChem number:24893588

Physical property data

1. Properties: off-white crystalline powder.

2. Density (g/mL, 20℃): 1.10

3. Relative vapor density (g/mL, air=1): Undetermined

4. Melting point (ºC): 72-75

5. Boiling point (ºC, normal pressure): Undetermined

6. Boiling point (ºC, 17mmHg): 176-177

7. Refractive index: 1.417

8. Flash point (ºC): 164

9. Specific rotation (º): Undetermined

10. Autoignition point or ignition temperature (ºC): Not determined

11. Vapor pressure (mmHg, ºC): Not determined

12. Saturated vapor pressure (kPa , ºC): Undetermined

13. Heat of combustion (KJ/mol): Undetermined

14. Critical temperature (ºC): Undetermined

15 . Critical pressure (KPa): Undetermined

16. Log value of oil-water (octanol/water) distribution coefficient: Undetermined

17. Explosion upper limit (%, V/V ): Undetermined

18. Lower explosion limit (%, V/V): Undetermined

19. Solubility: Slightly soluble in water, soluble in alcohol, ether, chloroform, Acids, most organic solvents.

Toxicological data

1. Acute toxicity: Rat oral LDLo: 500 mg/kg; Rat peritoneal cavity LD50: 620mg/kg; Mouse oral LD50: 800mg/kg; Mouse peritoneal cavity LD50: 200mg/kg; 2. Others Dose toxicity: rat peritoneal cavity TDLo: 1800mg/kg/9D-I;

Ecological data

This substance is slightly hazardous to water.

Molecular structure data

1. Molar refractive index: 47.31

2. Molar volume (cm3/mol): 139.0

3. Isotonic specific volume (90.2K ): 354.3

4. Surface tension (dyne/cm): 42.1

5. Dielectric constant:

6. Dipole moment (10-24cm3):

7. Polarizability: 18.75

Compute chemical data

1. Reference value for hydrophobic parameter calculation (XlogP): None

2. Number of hydrogen bond donors: 0

3. Number of hydrogen bond acceptors: 2

4. Number of rotatable chemical bonds: 2

5. Number of tautomers: none

6. Topological molecule polar surface area 20.3

7. Number of heavy atoms: 11

8. Surface charge: 0

9. Complexity: 126

10. Number of isotope atoms: 0

11. Determine the number of atomic stereocenters: 0

12. Uncertain number of atomic stereocenters: 0

13. Determine the number of chemical bond stereocenters: 0

14. Number of uncertain chemical bond stereocenters: 0

15. Number of covalent bond units: 1

Properties and stability

Avoid contact with air and light, and avoid contact with strong oxidants, strong alkali, and air.

Storage method

Store in a cool, ventilated warehouse. Keep away from fire and heat sources. The packaging must be sealed and must not come into contact with air. They should be stored separately from oxidants, alkalis, etc. and avoid mixed storage. Equipped with the appropriate variety and quantity of fire equipment. Suitable materials should be available in the storage area to contain spills.

Synthesis method

Using N,N-dimethylaniline as raw material, it can be produced by two methods. (1) Use methenamine to react to form methylene-N,N-dimethylaminobenzylamine, which is translocated to form N,N-dimethylbenzylamine, and then hydrolyzed to obtain the product. (2) React with dimethylformamide in the presence of phosphorus oxychloride. In addition, there is a laboratory preparation method that uses N,N-dimethylaniline, sodium nitrite, and formaldehyde as raw materials.

Purpose

It is used as a dye intermediate, as well as a reagent for the determination of urobilin, indole, alkaloids, etc. and a chromatographic analysis reagent.

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