Epoxy curing agent Knowledge p-Cresol p-Cresol

p-Cresol p-Cresol

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Structural formula of p-cresol

Structural formula

Business number 02TG
Molecular formula C7H8O
Molecular weight 108.14
label

p-cresol,

p-methylphenol,

To Kreisseur,

2-methylphenol,

4-Cresol,

1-hydroxy-4-methylbenzene,

1-Methyl-4-hydroxybenzene,

4-Cresol,

4-Methyl-phenol,

4-Methylphenol

Numbering system

CAS number:106-44-5

MDL number:MFCD00002376

EINECS number:203-398-6

RTECS number:GO6475000

BRN number:1305151

PubChem ID:None

Physical property data

1. Characteristics: colorless crystals with aromatic odor. [1]

2. Melting point (℃): 35.5[2]

3. Boiling point (℃): 201.8 [3]

4. Relative density (water = 1): 1.039[4]

5. Relative vapor density (Air=1): 3.72[5]

6. Saturated vapor pressure (kPa): 0.13 (53℃)[6]

7. Heat of combustion (kJ/mol): -3695.1[7]

8. Critical temperature (℃): 431.6[8]

9. Critical pressure (MPa): 5.51[9]

10. Octanol/water partition coefficient: 1.94[ 10]

11. Flash point (℃): 86 (CC) [11]

12. Ignition temperature (℃) :559[12]

13. Explosion upper limit (%): 1.1 (150℃)[13]

14 .Lower explosion limit (%): 7.6[14]

15. Solubility: Slightly soluble in water, soluble in ethanol, ether, chloroform, alkali, etc. [15]

16. Viscosity (mPa·s, 20ºC): 18.95

17. Heat of evaporation (KJ/kg, b.p.): 438.9

18. Heat of fusion (KJ/mol): 12.27

19. Specific heat capacity (KJ/(kg·K), 9~28ºC, constant pressure): 2.04

20. Conductivity (S/m, 25ºC): 1.378×10-8

21. Solubility (%, 25ºC, water): 2.1

22. Refractive index at room temperature (n25): 1.531640

23. Relative density (25℃, 4℃): 1.017941

24. Eccentricity factor: 0.513

25. Gas phase standard combustion heat (enthalpy) (kJ·mol-1): -3772.55

26. Gas phase standard claimed heat (enthalpy) (kJ·mol-1): -125.35

27. Gas phase standard entropy (J· mol-1·K-1): 350.86

28. Gas phase standard free energy of formation (kJ·mol-1): -31.5

29. Gas phase standard hot melt (J·mol-1·K-1): 124.97

30. Crystal phase standard combustion heat (enthalpy) (kJ·mol-1): -3698.61

31. Crystal phase standard claim heat (enthalpy) (kJ· mol-1): -199.28

32. Crystal phase standard entropy (J·mol-1·K-1): 167.2

33. Crystal phase standard formation free energy (kJ·mol-1): -50.96

34. Crystal phase standard hot melt (J·mol-1·KAfter the toluene and water are evaporated, the 93-104°C fraction is cut at a vacuum of 0.094 MPa to obtain p-cresol with a purity of 95%.

(2) Toluidine diazo hydrolysis method

  P-toluidine and sulfuric acid produce p-toluidine sulfate, which is diazotized with sodium nitrite at 0 to 5°C. The diazonium salt is then heated and hydrolyzed in dilute sulfuric acid, and the oil is separated with steam. Separate the oil layer and add it to 1% sodium hydroxide, then decolorize and filter, add concentrated sulfuric acid to pH=1, then separate the water layer, add zinc powder and sulfuric acid, neutralize with sodium carbonate until neutral, and separate. The oily substance is washed with water and then distilled under reduced pressure to obtain the finished product.

(3) It can be obtained by alkali melting sodium p-toluenesulfonate and then acidification.

Purpose

1.GB 2760–1996 stipulates that edible spices are allowed to be used. It is used in organic synthesis and is also a raw material for the manufacture of antioxidant 2,6-di-tert-butyl-p-cresol and rubber antioxidant. At the same time, it is an important basic raw material for the production of pharmaceutical TMP and dye colicidine sulfonic acid.

2. Used as analytical reagent. Used in organic synthesis. Also used as a fungicide and antifungal agent.

3. Mainly used in adhesives to make phenolic resin. It is also used as a raw material for the antioxidant 2,6-di-tert-butyl-p-cresol. It is used as a disinfectant in medicine, and trimethoxybenzaldehyde is used as a synergist in the synthesis of sulfa drugs. In addition, it can also be used to make paints, plasticizers, flotation agents, cresolic acid dyes and pesticides, etc.

4. Used in organic synthesis and as fungicides and fungicides. [28]

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