Epoxy curing agent Knowledge 1-Dodecylamine 1-Dodecylamine

1-Dodecylamine 1-Dodecylamine

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1-Dodecylamine structural formula

Structural formula

Business number 03J1
Molecular formula C12H27N
Molecular weight 185.35
label

1-aminododecane,

Dodecanylamine,

dodecylamine,

Dodecyl primary amine,

Laureamine,

dodecylamine,

n-dodecylamine,

1-Aminododecane,

Laurylamine,

linear compound

Numbering system

CAS number:124-22-1

MDL number:MFCD00008154

EINECS number:204-690-6

RTECS number:JR6475000

BRN number:1633576

PubChem ID:None

Physical property data

1. Properties: white waxy solid

2. Melting point: 28.20℃

3. Boiling point: 259℃

4. Relative density: 0.8015 (20/4℃)

5. Refractive index: 1.4421

6. Solubility: Soluble in ethanol, ether, benzene, chloroform and carbon tetrachloride, hardly soluble in water

Toxicological data

1. Skin/eye irritation: Rabbit skin standard Drez eye dye test: 750ug/24H has a serious irritating effect on the skin.

Standard Drez eye dye test on rabbit eyes: 50ug/24H has a serious irritating effect on the eyes.

2. Acute toxicity: rat oral LD5O: 1020mg/kg; mouse oral LD5O: 1160mg/kg; mouse peritoneal cavity LD5O: 50mg/kg

Ecological data

None

Molecular structure data

1. Molar refractive index: 61.17

2. Molar volume (cm3/mol): 230.2

3. Isotonic specific volume (90.2K ): 538.6

4. Surface tension (dyne/cm): 29.9

5. Polarizability (10-24cm3): 24.25

Compute chemical data

1. Reference value for hydrophobic parameter calculation (XlogP): None

2. Number of hydrogen bond donors: 1

3. Number of hydrogen bond acceptors: 1

4. Number of rotatable chemical bonds: 10

5. Number of tautomers: none

6. Topological molecule polar surface area 26

7. Number of heavy atoms: 13

8. Surface charge: 0

9. Complexity: 81.2

10. Number of isotope atoms: 0

11. Determine the number of atomic stereocenters: 0

12. Uncertain number of atomic stereocenters: 0

13. Determine the number of chemical bond stereocenters: 0

14. Number of uncertain chemical bond stereocenters: 0

15. Number of covalent bond units: 1

Properties and stability

This product is toxic, can irritate the skin, can causesubacute dermatitis, and has a certain stimulating effect on the central nervous system. Production equipment should be sealed to prevent escape, leakage, dripping and leakage, and operators should wear��Protective equipment. See n-butylamine for other requirements.
 

Storage method

Storage: sealed and stored at room temperature.

Our country uses galvanized iron drums for sealed packaging, and Japan uses 200L steel drums, with a net weight of 160kg. During storage and transportation, the barrel mouth should be upward, stored in a cool and ventilated place, away from fire and heat sources.

Synthesis method

Brief description of the production method: Use lauric acid as raw material and react with ammonia gas in the presence of catalyst silica gel. The product is washed with water, dried and distilled under reduced pressure to obtain lauryl nitrile. Laurel nitrile is hydrogenated under the catalysis of active nickel, which is reduced to obtain dodecylamine. Add lauryl nitrile to the autoclave, add an appropriate amount of active nickel, and replace the indoor air with nitrogen. Heat to 80°C with stirring, repeatedly charge with hydrogen until no longer absorbed, and keep warm for 3 hours. Cool and distill the crude product under reduced pressure to obtain dodecaamine.

Purpose

Organic synthesis intermediate, used in the production of textile and rubber additives. It can also be used to prepare ore flotation agents, dodecyl quaternary ammonium salts, bactericides, insecticides, emulsifiers, detergents, and special disinfectants that prevent and treat skin burns, nourish body fluids, and provide antibacterial effects.

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